反应条件
1.1: dichloro-acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dimethyl sulfoxide; toluene / 6 h / 23 °C / Inert atmosphere 2.1: n-butyllithium; zinc(II) chloride / Inert atmosphere 2.2: Inert atmosphere 3.1: ammonium cerium (IV) nitrate; water / methanol / 6 h / 0 °C / Inert atmosphere View Scheme
参考文献
Nguyen, Henry; Ma, Gil; Gladysheva, Tatiana; Fremgen, Trisha; Romo, Daniel
Journal of Organic Chemistry, 2011 , vol. 76, # 1 p. 2 - 12