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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
123990-98-7
合成路线
（共 8 条）
930-68-7
2-环己烯-1-酮
+
100-51-6
苯甲醇
→
反应条件
123990-98-7
反应条件
4-(N,N-dimethlyamino)pyridine; lithium perchlorate T=-20°C; Michael reaction; P=1520000 Torr; 85 h;
参考文献
Hayashi, Yujiro; Nishimura, Koichi
Chemistry Letters, 2002 , # 3 p. 296 - 297
84029-18-5
→
反应条件
123990-98-7
反应条件
1: LAH 2: CrO3; H2SO4 / acetone / 0.08 h / 20 °C View Scheme
参考文献
Crotti, Paolo; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro; Marianucci, Francesco; Renzi, Gabriele; Amici, Giuseppina; Roselli, Graziella
Tetrahedron, 2000 , vol. 56, # 38 p. 7513 - 7524
445481-11-8
→
反应条件
2987-06-6
4-(苄氧基)环己酮
+
123990-98-7
反应条件
chromium(VI) oxide; sulfuric acid in acetone T=20°C; Oxidation; 0.0833333 h;
参考文献
Crotti, Paolo; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro; Marianucci, Francesco; Renzi, Gabriele; Amici, Giuseppina; Roselli, Graziella
Tetrahedron, 2000 , vol. 56, # 38 p. 7513 - 7524
84049-33-2
→
反应条件
123990-98-7
反应条件
1: 60 mg / LiAlH4 / diethyl ether / 2 h / Ambient temperature; or with LiAlH4/12-crown-4 2: 20 mg / CrO3 / acetone View Scheme
参考文献
Chini, Marco; Crotti, Paolo; Flippin, Lee A.; Macchia, Franco
Journal of Organic Chemistry, 1990 , vol. 55, # 14 p. 4265 - 4272
127383-50-0
→
反应条件
123990-98-7
反应条件
1: t-BuOK / benzene / Ambient temperature 2: 60 mg / LiAlH4 / diethyl ether / 2 h / Ambient temperature; or with LiAlH4/12-crown-4 3: 20 mg / CrO3 / acetone View Scheme
参考文献
Chini, Marco; Crotti, Paolo; Flippin, Lee A.; Macchia, Franco
Journal of Organic Chemistry, 1990 , vol. 55, # 14 p. 4265 - 4272
67-56-1
甲醇
+
84029-18-5
→
反应条件
2987-06-6
4-(苄氧基)环己酮
+
123990-98-7
+
127383-54-4
+
127383-53-3
反应条件
deuterium T=37.5°C; Ring cleavage; P=100 Torr; Irradiation; Product distribution; Further Variations:ReagentsPressures;
参考文献
Crotti, Paolo; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro; Marianucci, Francesco; Renzi, Gabriele; Amici, Giuseppina; Roselli, Graziella
Tetrahedron, 2000 , vol. 56, # 38 p. 7513 - 7524
67-56-1
甲醇
+
84049-33-2
→
反应条件
2987-06-6
4-(苄氧基)环己酮
+
123990-98-7
+
127383-55-5
+
127383-54-4
反应条件
deuterium T=37.5°C; Ring cleavage; P=100 Torr; Irradiation; Product distribution; Further Variations:ReagentsPressures;
参考文献
Crotti, Paolo; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro; Marianucci, Francesco; Renzi, Gabriele; Amici, Giuseppina; Roselli, Graziella
Tetrahedron, 2000 , vol. 56, # 38 p. 7513 - 7524
67-56-1
甲醇
+
84029-20-9
→
反应条件
36713-55-0
+
123990-98-7
反应条件
deuterium T=37.5°C; Ring cleavage; P=100 Torr; Irradiation; Product distribution; Further Variations:ReagentsPressures;
参考文献
Crotti, Paolo; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro; Marianucci, Francesco; Renzi, Gabriele; Amici, Giuseppina; Roselli, Graziella
Tetrahedron, 2000 , vol. 56, # 38 p. 7513 - 7524
