1: HCl gas / CH2Cl2 2: monoperphthalic acid / diethyl ether 3: 0.25 g / t-BuOK / diethyl ether; 2-methyl-propan-2-ol / 2.5 h / 20 °C View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, # 6 p. 1225 - 1231
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1375 - 1382
1: monoperphthalic acid / diethyl ether 2: 0.25 g / t-BuOK / diethyl ether; 2-methyl-propan-2-ol / 2.5 h / 20 °C View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, # 6 p. 1225 - 1231
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1375 - 1382
1,1-dibromo ethane; magnesium in tetrahydrofuran 4 h; Heating; Yield given. Yields of byproduct given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 10 p. 2160 - 2162
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2397 - 2399
Rh(I)Cl(CO)(PMe3)2 P=760 Torr; 5 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
Rh(I)Cl(CO)(PMe3)2 P=760 Torr; 5 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
Rh(I)Cl(CO)(PMe3)2 P=760 Torr; 5 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
