1: 1-bromo-butane With iodine; magnesium in diethyl ether T=60°C; 1 h; 2: 1-bromo-decane With 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; ferrous acetate in diethyl ether T=20°C; Kumada coupling reaction; 0.25 h; Further stages. Title compound not separated from byproducts.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 7 p. 1015 - 1018
Fe3O4Rh; hydrazine hydrate in ethanol T=80°C; 22 h; Inert atmosphere;
参考文献
Jang, Youngjin; Kim, Seyoung; Jun, Samuel Woojoo; Kim, Byung Hyo; Hwang, Sunhwan; Song, In Kyu; Kim, B. Moon; Hyeon, Taeghwan
Chemical Communications, 2011 , vol. 47, # 12 p. 3601 - 3603
