NaOH in methanol; water
amine was added to soln. of NaOH in MeOH; cooled at 10°C in ice bath; CS2 was added dropwise with stirring; bath removed; aq. soln. of ZnCl2 was slowly added with stirring; filtered; residue washed (H2O); dried in vac. at room temp.; elem. anal.;
参考文献
Memon, Ashfaq A.; Afzaal, Mohammad; Malik, Mohammad A.; Nguyen, Chinh Q.; O'Brien, Paul; Raftery, Jim
Dalton Transactions, 2006 , # 37 p. 4499 - 4505
