1,1,2,2-四氟-1,2-二溴乙烷合成路线 （共 103 条）
反应条件
aluminium trichloride T=50 - 55°C; 22 h; Further byproducts given;
参考文献
Hemer,I.; Posta,A.
Journal of Fluorine Chemistry, 1984 , vol. 26, p. 467
反应条件
in gas
byproducts: C2F4, NO, CO; Irradiation (UV/VIS); on UV irradiation of gaseous mixture with BrCF2CF2Br at 0°C;;
参考文献
Seel, F.; Roeschenthaler, G.-V.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1971 , vol. 386, p. 297 - 315
Full Text Show Details
Gmelin Handbook: Co: Org.Verb.1, 1.1.5.3.1.3, page 176 - 184
反应条件
in further solvent(s)
byproducts: C2F4, NO, CO; Irradiation (UV/VIS); on UV photolysis in BrCF2CF2Br at -10°C;;
参考文献
Seel, F.; Roeschenthaler, G.-V.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1971 , vol. 386, p. 297 - 315
Full Text Show Details
Gmelin Handbook: Co: Org.Verb.1, 1.1.5.3.1.3, page 176 - 184
反应条件
n-butyllithium; diisopropylamine in tetrahydrofuran; hexane
T=-75°C;
参考文献
Schlosser, Manfred; Heiss, Christophe
European Journal of Organic Chemistry, 2003 , # 23 p. 4618 - 4624
反应条件
Faigl mix in tetrahydrofuran; hexane
T=-100°C; 2 h;
参考文献
Heiss, Christophe; Marzi, Elena; Schlosser, Manfred
European Journal of Organic Chemistry, 2003 , # 23 p. 4625 - 4629
反应条件
(NH4)2S2O8; sodium formate in N,N-dimethyl-formamide
T=40°C; 3.5 h; other acetylenes; stereoselectivity; Mechanism;
参考文献
Hu, Chang-Ming; Qiu, Yao-Ling; Qing, Feng-Ling
Journal of Fluorine Chemistry, 1991 , vol. 51, # 2 p. 295 - 298
反应条件
aluminium trichloride
T=50 - 55°C; 22 h; Further byproducts given;
参考文献
Hemer,I.; Posta,A.
Journal of Fluorine Chemistry, 1984 , vol. 26, p. 467
反应条件
aluminium trichloride
T=50 - 55°C; 22 h; Further byproducts given;
参考文献
Hemer,I.; Posta,A.
Journal of Fluorine Chemistry, 1984 , vol. 26, p. 467
反应条件
bromine(I) fluorosulfate; SbF5; epoxysulfonyl fluoride
T=20°C; 2 h;
参考文献
Fokin, A. V.; Studnev, Yu. N.; Rapkin, A. I.; Tatarinov, A. S.; Seryanov, Yu. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 7 p. 1495 - 1498
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 7 p. 1635 - 1638
反应条件
triethylamine in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=40°C; 72 h;
参考文献
Li, Xing-ya; Pan, He-qi; Jiang, Xi-kui
Tetrahedron Letters, 1987 , vol. 28, # 32 p. 3699 - 3702
