1,1,2,2-四氟-1,2-二溴乙烷合成路线 (共 103 条)
反应条件
potassium hydroxide in methanol
参考文献
The Dow Chemical Company
Patent: US5023380 A1, 1991 ;
反应条件
T=1120°C; single-pulse shock-tube studies on the decomposition of 1,2-dibromoperfluoroethane; Product distribution;
参考文献
Tsang, Wing
Journal of Physical Chemistry, 1984 , vol. 88, # 13 p. 2812 - 2817
反应条件
T=30°C; Irradiation;
参考文献
Journal of Fluorine Chemistry, , vol. 88, # 2 p. 153 - 168
反应条件
propane-1-thiol in N,N-dimethyl-formamide T=40°C; 4 h; Yield given. Yields of byproduct given;
参考文献
Rico, I.; Wakselman, C.
Journal of Fluorine Chemistry, 1982 , vol. 20, p. 759 - 764
参考文献
Pfizer Inc.
Patent: US6492383 B1, 2002 ;
反应条件
1: phenol With potassium hydroxide in methanol Metallation; 2: 1,2-dibromo-1,1,2,2-tetrafluoroethane in dimethyl sulfoxide T=60°C; Etherification; 6 h;
参考文献
Zhang, Sen; Liu, Hao; Deng, Yan; Huang, Xiaoyu
Journal of Fluorine Chemistry, 2012 , vol. 133, p. 184 - 189
反应条件
caesium carbonate in dimethyl sulfoxide T=50°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 48, # 42 p. 7516 - 7519
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide 6 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 25, # 43 p. 4937 - 4940
参考文献
Chang, Seung Wook; Ayothi, Ramakrishnan; Bratton, Daniel; Yang, Da; Felix, Nelson; Cao, Heidi B.; Deng, Hai; Ober, Christopher K.
Journal of Materials Chemistry, 2006 , vol. 16, # 15 p. 1470 - 1474
反应条件
aluminium trichloride; methyl iodide
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 949 - 956