8-(4-氯苯氧基)-1-辛烯-2-醇合成路线 （共 6 条）
反应条件
sodium tetrahydroborate; silica gel in diethyl ether 18 h; Ambient temperature;
参考文献
Crilley, Martine M. L.; Edmunds, Andrew J. F.; Eistetter, Klaus; Golding, Bernard T.
Tetrahedron Letters, 1989 , vol. 30, # 7 p. 885 - 888
反应条件
aluminium hydride in diethyl ether Yield given;
参考文献
Crilley, Martine M. L.; Edmunds, Andrew J. F.; Eistetter, Klaus; Golding, Bernard T.
Tetrahedron Letters, 1989 , vol. 30, # 7 p. 885 - 888
反应条件
1: 63 percent / SOCl2 / 18 h / from 0 deg C to room temp. 2: 60 percent / NaBH4-silica / diethyl ether / 18 h / Ambient temperature View Scheme
参考文献
Crilley, Martine M. L.; Edmunds, Andrew J. F.; Eistetter, Klaus; Golding, Bernard T.
Tetrahedron Letters, 1989 , vol. 30, # 7 p. 885 - 888
反应条件
1: NaOEt / ethanol 2: 1.) NaH, 2.) Red-AlR / 1.) toluene, reflux, 2.) 45 deg C View Scheme
参考文献
Prasad; Estermann; Chen; Repic; Hardtmann
Tetrahedron Asymmetry, 1990 , vol. 1, # 7 p. 421 - 424
反应条件
sodium hydride; sodium bis(2-methoxyethoxy)aluminium dihydride 1.) toluene, reflux, 2.) 45 deg C; Multistep reaction;
参考文献
Prasad; Estermann; Chen; Repic; Hardtmann
Tetrahedron Asymmetry, 1990 , vol. 1, # 7 p. 421 - 424
反应条件
1: 49 percent / t-butylhydroperoxide, titanium isopropoxide, diethyl L-(+)-tartrate / -20 deg C, 3 h. then room temp., 1 h. 2: 1.) NaIO4; 2.) NaHCO3 / 1.) RuCl3 / 1.) CCl4, CH3CN, H2O, room temp., 7 h.; 2.) DMF, room temp. View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 7 p. 885 - 888
