8-(4-氯苯氧基)-2-亚甲基辛酸合成路线 （共 3 条）
反应条件
sodium hydroxide in methanol 18 h; Ambient temperature;
参考文献
Crilley, Martine M. L.; Edmunds, Andrew J. F.; Eistetter, Klaus; Golding, Bernard T.
Tetrahedron Letters, 1989 , vol. 30, # 7 p. 885 - 888
反应条件
1: 63 percent / SOCl2 / 18 h / from 0 deg C to room temp. 2: 60 percent / NaBH4-silica / diethyl ether / 18 h / Ambient temperature 3: 49 percent / t-butylhydroperoxide, titanium isopropoxide, diethyl L-(+)-tartrate / -20 deg C, 3 h. then room temp., 1 h. 4: 1.) NaIO4; 2.) NaHCO3 / 1.) RuCl3 / 1.) CCl4, CH3CN, H2O, room temp., 7 h.; 2.) DMF, room temp. View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 7 p. 885 - 888
反应条件
1: 63 percent / SOCl2 / 18 h / from 0 deg C to room temp. 2: 60 percent / NaBH4-silica / diethyl ether / 18 h / Ambient temperature View Scheme
参考文献
Crilley, Martine M. L.; Edmunds, Andrew J. F.; Eistetter, Klaus; Golding, Bernard T.
Tetrahedron Letters, 1989 , vol. 30, # 7 p. 885 - 888
