RhCl(PPh3)3 in diethyl ether T=20°C; P=9375940 Torr; 96 h;
参考文献
Colin, Sylvie; Vaysse-Ludot, Lucile; Lecouve, Jean-Pierre; Maddaluno, Jacques
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 24 p. 4505 - 4511
[rhodium(I)chloride(triphenylphosphine)3] in diethyl ether High Pressure; Ar; pinacolborane (2 equiv.) slowly added to a soln. of BrC3H4Br and RhCl(P(C6H5)3)3 at 20°C, placed under 13 kbar for 72 h; solvent removed (vac.), chromy. (silica gel, 80:20 heptane-ethyl acetate);
参考文献
Colin, Sylvie; Vaysse-Ludot, Lucile; Lecouve, Jean-Pierre; Maddaluno, Jacques
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 24 p. 4505 - 4511
[rhodium(I)chloride(triphenylphosphine)3] in tetrahydrofuran High Pressure; Ar; pinacolborane (2 equiv.) slowly added to a soln. of BrC3H4Br and RhCl(P(C6H5)3)3 at 20°C, placed under 13 kbar for 72 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 24 p. 4505 - 4511
NiI2*3.5H2O; C5H5N; Zn in further solvent(s) in 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone in the presence ofNiI2*3.5H2O, C5H5N, NaI and Zn dust; heated at 60°C under air;
参考文献
Everson, Daniel A.; Jones, Brittany A.; Weix, Daniel J.
Journal of the American Chemical Society, 2012 , vol. 134, # 14 p. 6146 - 6159
