5-溴-7-氟-2,3-二氢-1H-茚-1-酮合成路线 (共 2 条)
反应条件
AlCl3, aluminium chloride; sodium chloride T=130 - 180°C; 1 h; Inert atmosphere;
参考文献
Aebi, Johannes; Binggeli, Alfred; Hertel, Cornelia; Konkar, Anish Ashok; Kuehne, Holger; Kuhn, Bernd; Maerki, Hans P.; Wang, Haiyan
Patent: US2013/18055 A1, 2013 ;
Location in patent: Paragraph 0324-0325 ;
反应条件
1.1: thionyl chloride / benzene / 12 h / Reflux; Inert atmosphere 1.2: 2 h / 20 °C / Inert atmosphere 2.1: AlCl3, aluminium chloride; sodium chloride / 1 h / 130 - 180 °C / Inert atmosphere View Scheme
参考文献
Aebi, Johannes; Binggeli, Alfred; Hertel, Cornelia; Konkar, Anish Ashok; Kuehne, Holger; Kuhn, Bernd; Maerki, Hans P.; Wang, Haiyan
Patent: US2013/18055 A1, 2013 ;