1,1’-二(联苯膦)二茂铁溴化钯(II)合成路线 (共 3 条)
反应条件
in acetone to suspn. of Pd-complex in acetone Fe-complex was added, stirred at roomtemp. for 2 h under inert atm.; vol. was reduced in vac., Et2O was added, stirred for 10 min, filtered, washed with Et2O, dried under vac.;
参考文献
Journal of Organometallic Chemistry, , vol. 637-639, p. 691 - 697
反应条件
in dichloromethane (Ar), stirring a soln. of palladium complex and silver salt in CH2Cl2 atroom temp. for 2 h in the dark;
参考文献
Neo, Yew Chin; Yeo, Jeremy Shu Lip; Low, Pauline Meng Neo; Chien, Sheau Wei; Mak, Thomas C.W; Vittal, Jagadese J; Hor, T.S.Andy
Journal of Organometallic Chemistry, 2002 , vol. 658, # 1-2 p. 159 - 168
反应条件
in dichloromethane (Ar), stirring a soln. of palladium complex and silver salt in CH2Cl2 atroom temp. for 2 h in the dark;
参考文献
Neo, Yew Chin; Yeo, Jeremy Shu Lip; Low, Pauline Meng Neo; Chien, Sheau Wei; Mak, Thomas C.W; Vittal, Jagadese J; Hor, T.S.Andy
Journal of Organometallic Chemistry, 2002 , vol. 658, # 1-2 p. 159 - 168