N-(三苯基正膦亚基)-1H-苯并三唑-1-甲胺合成路线 （共 14 条）
反应条件
n-butyllithium 1.) hexane, THF, -78 deg C, 1 h, 2.) hexane, THF, RT, 20 h; Yield given. Multistep reaction;
参考文献
F. HOFFMANN-LA ROCHE AG
Patent: WO2009/77334 A1, 2009 ;
Location in patent: Page/Page column 96-97 ;
WO 2009/077334 A1
反应条件
hydrogenchloride
1.) THF/diethyl ether, 20 min, rt.; 2.) diethyl ether, 1h;
参考文献
Katritzky, Alan R.; Jiang, Jinlong; Urogdi, Laszlo
Tetrahedron Letters, 1989 , vol. 30, # 25 p. 3303 - 3306
反应条件
1) THF, RT, 5h, 2) THF, RT, 12h; Yield given. Multistep reaction;
参考文献
Katritzky, Alan R.; Jiang, Jinglong; Urogdi, Laszlo
Synthesis, 1990 , # 7 p. 565 - 567
反应条件
hydrogenchloride
1.) THF/diethyl ether, 20 min, rt.; 2.) diethyl ether, 1h;
参考文献
Katritzky, Alan R.; Jiang, Jinlong; Urogdi, Laszlo
Tetrahedron Letters, 1989 , vol. 30, # 25 p. 3303 - 3306
