N,N-二甲基乙基醛烷胺络合物溶液合成路线 （共 3 条）
反应条件
1: AlCl3, aluminium chloride; lithium aluminium tetrahydride in diethyl ether T=-10°C; 0.00833333 h; 2: dimethylethylamine in diethyl ether T=-10°C; 5 h; Product distribution / selectivity;
参考文献
WO2007/136184 A1, ;
Page/Page column 17-18; 18-19 ;
反应条件
in neat (no solvent) T=131°C; Inert atmosphere;
参考文献
Humphries, Terry D.; Munroe, Keelie T.; Decken, Andreas; McGrady, G. Sean
Dalton Transactions, 2013 , vol. 42, # 19 p. 6965 - 6978
反应条件
titanium(IV) isopropylate in 1,2,5-trimethyl-benzene byproducts: (CH3)2N(C2H5), H2; 164°C; transmission electron microscopy; elem. anal.;
参考文献
Xenidou, Theodora C.; Prud'Homme, Nathalie; Vahlas, Constantin; Markatos, Nicholas C.; Boudouvis, Andreas G.
Journal of the Electrochemical Society, 2010 , vol. 157, # 12 p. D633-D641
