3-羟基-3,4,5,7-四甲氧基黄酮合成路线 (共 29 条)
反应条件
in benzene T=37°C; Decomposition; radical-capturing; 83 h; Product distribution; Further Variations:reaction time;
参考文献
Ishikawa, Takahiro; Takagi, Michiyo; Kanou, Mamiko; Kawai, Shingo; Ohashi, Hideo
Bioscience, Biotechnology and Biochemistry, 2000 , vol. 64, # 1 p. 173 - 177
反应条件
boron tribromide in dichloromethane 6 h; Heating;
参考文献
Chu, Han-Wei; Wu, Huan-Ting; Lee, Yean-Jang
Tetrahedron, 2004 , vol. 60, # 11 p. 2647 - 2655
参考文献
v. Kostanecki; Lampe; Tambor
Chemische Berichte, 1904 , vol. 37, p. 1403
反应条件
in benzene T=37°C; Decomposition; radical-capturing; 83 h; Product distribution; Further Variations:reaction time;
参考文献
Ishikawa, Takahiro; Takagi, Michiyo; Kanou, Mamiko; Kawai, Shingo; Ohashi, Hideo
Bioscience, Biotechnology and Biochemistry, 2000 , vol. 64, # 1 p. 173 - 177
反应条件
in benzene T=37°C; Decomposition; radical-capturing; Product distribution;
参考文献
Ishikawa, Takahiro; Takagi, Michiyo; Kanou, Mamiko; Kawai, Shingo; Ohashi, Hideo
Bioscience, Biotechnology and Biochemistry, 2000 , vol. 64, # 1 p. 173 - 177
反应条件
1: 96 percent / K2CO3 / acetone / 1 h / Heating 2: 99 percent / BBr3 / CH2Cl2 / 0.5 h / 0 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 11 p. 2647 - 2655
反应条件
hydrogenchloride in water
1 h; Reflux;
参考文献
Wang, Zhonglei; Yang, Liyan; Cui, Shuai; Liang, Yingxi; Zhang, Xiaohua
Molecules, 2014 , vol. 19, # 4 p. 4791 - 4801
反应条件
3,3-dimethyldioxirane in dichloromethane; acetone
T=0 - 20°C; 0.5 h;
参考文献
Chu, Han-Wei; Wu, Huan-Ting; Lee, Yean-Jang
Tetrahedron, 2004 , vol. 60, # 11 p. 2647 - 2655
反应条件
aluminum tri-bromide in acetonitrile
T=0°C; 1 h;
参考文献
De La Torre, Maria D.L.; Tome, Augusto C.; Silva, Artur M.S.; Cavaleiro, Jose A.S.
Tetrahedron Letters, 2002 , vol. 43, # 26 p. 4617 - 4620
反应条件
aluminum tri-bromide in acetonitrile
T=0°C; 1.5 h;
参考文献
De La Torre, Maria D. L.; Rodrigues, Andrea G. P.; Tome, Augusto C.; Silva, Artur M. S.; Cavaleiro, Jose A. S.
Tetrahedron, 2004 , vol. 60, # 16 p. 3581 - 3592