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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
124493-84-1
合成路线
（共 12 条）
124-63-0
甲烷磺酰氯
+
101796-28-5
→
反应条件
124493-84-1
反应条件
pyridine in dichloromethane 48 h; Ambient temperature;
参考文献
Terochem Laboratories Limited
Patent: US5410033 A1, 1995 ;
76-83-5
三苯基氯甲烷
+
124-63-0
甲烷磺酰氯
+
1463-10-1
5-甲基尿甙
→
反应条件
124493-84-1
反应条件
pyridine 1.) a) 0 deg C, overnight, b) 70 deg C, 3 h, 2.) a) 0 deg C, 1 h, b) RT, overnight; Yield given. Multistep reaction;
参考文献
Huang; Chen; Wang; Kim; Warshaw; Armstrong; Zhu; Chou; Watanabe; Matulic-Adamic; Su; Fox; Polsky; Baron; Gold; Hardy; Zuckerman
Journal of Medicinal Chemistry, 1991 , vol. 34, # 5 p. 1640 - 1646
76-83-5
三苯基氯甲烷
→
反应条件
124493-84-1
反应条件
1: pyridine / 20 °C 2: 5 h / 0 °C View Scheme
参考文献
Haraguchi, Kazuhiro; Itoh, Yoshiharu; Takeda, Shingo; Honma, Yosuke; Tanaka, Hiromichi; Nitanda, Takao; Baba, Masanori; Dutschman, Ginger E.; Cheng, Yung-Chi
Nucleosides, Nucleotides and Nucleic Acids, 2004 , vol. 23, # 4 p. 647 - 654
1463-10-1
5-甲基尿甙
→
反应条件
124493-84-1
反应条件
1: pyridine / 20 °C 2: 5 h / 0 °C View Scheme
参考文献
Haraguchi, Kazuhiro; Itoh, Yoshiharu; Takeda, Shingo; Honma, Yosuke; Tanaka, Hiromichi; Nitanda, Takao; Baba, Masanori; Dutschman, Ginger E.; Cheng, Yung-Chi
Nucleosides, Nucleotides and Nucleic Acids, 2004 , vol. 23, # 4 p. 647 - 654
124493-84-1
→
反应条件
5964-41-0
5'-O-三苯甲基-2',3'-去氢胸苷
反应条件
lithium telluride in tetrahydrofuran 48 h; Ambient temperature;
参考文献
Clive, Derrick L. J.; Wickens, Philip L.; Sgarbi, Paulo W. M.
Journal of Organic Chemistry, 1996 , vol. 61, # 21 p. 7426 - 7437
124493-84-1
→
反应条件
128269-50-1
反应条件
1: 95 percent / 1 N NaOH / ethanol / 3 h / 60 °C 2: 30 percent / LiN3 / ethanol / 2 h / Heating View Scheme
参考文献
Huang; Chen; Wang; Kim; Warshaw; Armstrong; Zhu; Chou; Watanabe; Matulic-Adamic; Su; Fox; Polsky; Baron; Gold; Hardy; Zuckerman
Journal of Medicinal Chemistry, 1991 , vol. 34, # 5 p. 1640 - 1646
124493-84-1
→
反应条件
132776-26-2
反应条件
1: 95 percent / 1 N NaOH / ethanol / 3 h / 60 °C 2: 20 percent / LiN3 / ethanol / 2 h / Heating 3: 47 percent / DAST / benzene / 2 h / Ambient temperature View Scheme
参考文献
Huang; Chen; Wang; Kim; Warshaw; Armstrong; Zhu; Chou; Watanabe; Matulic-Adamic; Su; Fox; Polsky; Baron; Gold; Hardy; Zuckerman
Journal of Medicinal Chemistry, 1991 , vol. 34, # 5 p. 1640 - 1646
124493-84-1
→
反应条件
132776-27-3
反应条件
1: 95 percent / 1 N NaOH / ethanol / 3 h / 60 °C 2: 20 percent / LiN3 / ethanol / 2 h / Heating 3: 47 percent / DAST / benzene / 2 h / Ambient temperature 4: 60 percent / 80percent aq. AcOH / 0.25 h / Heating View Scheme
参考文献
Huang; Chen; Wang; Kim; Warshaw; Armstrong; Zhu; Chou; Watanabe; Matulic-Adamic; Su; Fox; Polsky; Baron; Gold; Hardy; Zuckerman
Journal of Medicinal Chemistry, 1991 , vol. 34, # 5 p. 1640 - 1646
124493-84-1
→
反应条件
127840-94-2
反应条件
1: 95 percent / 1 N NaOH / ethanol / 3 h / 60 °C 2: 30 percent / LiN3 / ethanol / 2 h / Heating 3: 65 percent / DAST / benzene / 2 h / Ambient temperature 4: 64 percent / 80percent aq. AcOH / 0.25 h / Heating View Scheme
参考文献
Huang; Chen; Wang; Kim; Warshaw; Armstrong; Zhu; Chou; Watanabe; Matulic-Adamic; Su; Fox; Polsky; Baron; Gold; Hardy; Zuckerman
Journal of Medicinal Chemistry, 1991 , vol. 34, # 5 p. 1640 - 1646
124493-84-1
→
反应条件
132776-25-1
反应条件
1: 95 percent / 1 N NaOH / ethanol / 3 h / 60 °C 2: 30 percent / LiN3 / ethanol / 2 h / Heating 3: 65 percent / DAST / benzene / 2 h / Ambient temperature View Scheme
参考文献
Huang; Chen; Wang; Kim; Warshaw; Armstrong; Zhu; Chou; Watanabe; Matulic-Adamic; Su; Fox; Polsky; Baron; Gold; Hardy; Zuckerman
Journal of Medicinal Chemistry, 1991 , vol. 34, # 5 p. 1640 - 1646
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