2-(1,4-二噁螺[4.5]-8-癸基)-乙胺合成路线 (共 4 条)
反应条件
lithium aluminium tetrahydride in diethyl ether 2 h; Ambient temperature; Yield given;
参考文献
Journal of Medicinal Chemistry, , vol. 36, # 6 p. 683 - 689
反应条件
1: Et3N / CH2Cl2 / 2 h / 0 °C 2: dimethylsulfoxide / 3 h / Heating 3: LAH / diethyl ether / 2 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 36, # 6 p. 683 - 689
反应条件
1: 90 percent / LAH / diethyl ether / 5 h / Ambient temperature 2: Et3N / CH2Cl2 / 2 h / 0 °C 3: dimethylsulfoxide / 3 h / Heating 4: LAH / diethyl ether / 2 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 36, # 6 p. 683 - 689
反应条件
1: dimethylsulfoxide / 3 h / Heating 2: LAH / diethyl ether / 2 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 36, # 6 p. 683 - 689