2,3,5,6-四溴噻吩并[3,2-b]噻吩合成路线 (共 6 条)
反应条件
bromine in carbon disulfide 23 h; Heating;
参考文献
Yui, Koji; Ishida, Hideki; Aso, Yoshio; Otsubo, Tetsuo; Ogura, Fumio; et al.
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 5 p. 1547 - 1555
反应条件
bromine; lithium diisopropyl amide in tetrahydrofuran; hexane 1.) -80 deg C, 5 min, 2.) -80 deg C to r.t.;
参考文献
Fuller, Lance S.; Iddon, Brian; Smith, Kevin A.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 22 p. 3465 - 3470
反应条件
bromine; acetic acid
参考文献
Youn, Jangdae; Huang, Peng-Yi; Huang, Yu-Wen; Chen, Ming-Chou; Lin, Yu-Jou; Huang, Hui; Ortiz, Rocio Ponce; Stern, Charlotte; Chung, Ming-Che; Feng, Chieh-Yuan; Chen, Liang-Hsiang; Facchetti, Antonio; Marks, Tobin J.
Advanced Functional Materials, 2012 , vol. 22, # 1 p. 48 - 60
反应条件
1: potassium carbonate 2: water; sodium hydroxide 3: bromine; acetic acid View Scheme
参考文献
Advanced Functional Materials, , vol. 22, # 1 p. 48 - 60
反应条件
acetic acid; zinc 1 h; Heating;
参考文献
Fuller, Lance S.; Iddon, Brian; Smith, Kevin A.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 22 p. 3465 - 3470
反应条件
1: Zn; AcOH
2: MeONa; CuO; KI
View Scheme
参考文献
Hergue, Noemie; Frere, Pierre; Roncali, Jean
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 2 p. 588 - 595