反应条件
n-butyllithium in tetrahydrofuran byproducts: LiCl; a soln. of phenylethyne in THF is cooled to -78°C and BuLi is slowly added with stirring, mixt. is stirred for 1 h, Ph3SnCl in THF is then added, mixt. is allowed to reach room temp. and stirred for a further hour; filtn. from LiCl, evapn.;
参考文献
Pelter, Andrew; Smith, Keith; Parry, David E.; Jones, Kevin D.
Australian Journal of Chemistry, 1992 , vol. 45, # 1 p. 57 - 70