栎精-3,5,7,3,4-五甲醚合成路线 （共 28 条）
反应条件
1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -15 - 0 °C / Inert atmosphere
2: sulfuric acid; acetic acid / 0.5 h / 80 °C
View Scheme
参考文献
Lee, Jae In; Park, Se Bin
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 4 p. 1379 - 1382
反应条件
1: triethylamine / dichloromethane / 0 - 20 °C
2: lithium diisopropyl amide / tetrahydrofuran / 1 h / -15 - 0 °C / Inert atmosphere
3: sulfuric acid; acetic acid / 0.5 h / 80 °C
View Scheme
参考文献
Lee, Jae In; Park, Se Bin
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 4 p. 1379 - 1382
参考文献
Herzig
Monatshefte fuer Chemie, 1912 , vol. 33, p. 697
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Watson
Journal of the Chemical Society, 1914 , vol. 105, p. 344
参考文献
Herzig
Monatshefte fuer Chemie, 1912 , vol. 33, p. 697
参考文献
Herzig
Monatshefte fuer Chemie, 1912 , vol. 33, p. 697
反应条件
aluminum tri-bromide in acetonitrile
T=0°C; 1 h;
参考文献
De La Torre, Maria D.L.; Tome, Augusto C.; Silva, Artur M.S.; Cavaleiro, Jose A.S.
Tetrahedron Letters, 2002 , vol. 43, # 26 p. 4617 - 4620
反应条件
aluminum tri-bromide in acetonitrile
T=0°C; 1.5 h;
参考文献
De La Torre, Maria D. L.; Rodrigues, Andrea G. P.; Tome, Augusto C.; Silva, Artur M. S.; Cavaleiro, Jose A. S.
Tetrahedron, 2004 , vol. 60, # 16 p. 3581 - 3592
反应条件
1: 99 percent / BBr3 / CH2Cl2 / 0.5 h / 0 °C
2: 89 percent / dimethyl dioxirane / acetone; CH2Cl2 / 0.83 h / 0 - 20 °C
View Scheme
参考文献
Chu, Han-Wei; Wu, Huan-Ting; Lee, Yean-Jang
Tetrahedron, 2004 , vol. 60, # 11 p. 2647 - 2655
