(E)-1-(2,4-二羟基-3-甲氧基苯基)-3-(4-甲氧基苯基)丙-2-烯-1-酮合成路线 （共 6 条）
反应条件
aluminium trichloride; N,N-dimethyl-aniline in dichloromethane T=5°C; 0.0833333 h;
参考文献
Raju, Vegesna S.; Subbaraju, Gottumukkala V.; Manhas, Maghar S.; Kaluza, Zbigniew; Bose, Ajay K.
Tetrahedron, 1992 , vol. 48, # 39 p. 8347 - 8352
反应条件
1: 82 percent / K2CO3 / 1,2-dimethoxy-ethane / 12 h / Heating 2: 65 percent / 10percent NaOH / ethanol / 240 h / 0 °C 3: 60 percent / AlCl3, N,N-dimethylaniline / CH2Cl2 / 0.08 h / 5 °C View Scheme
参考文献
Raju, Vegesna S.; Subbaraju, Gottumukkala V.; Manhas, Maghar S.; Kaluza, Zbigniew; Bose, Ajay K.
Tetrahedron, 1992 , vol. 48, # 39 p. 8347 - 8352
反应条件
1: 60 percent / triflic acid / 192 h / Ambient temperature 2: 82 percent / K2CO3 / 1,2-dimethoxy-ethane / 12 h / Heating 3: 65 percent / 10percent NaOH / ethanol / 240 h / 0 °C 4: 60 percent / AlCl3, N,N-dimethylaniline / CH2Cl2 / 0.08 h / 5 °C View Scheme
参考文献
Raju, Vegesna S.; Subbaraju, Gottumukkala V.; Manhas, Maghar S.; Kaluza, Zbigniew; Bose, Ajay K.
Tetrahedron, 1992 , vol. 48, # 39 p. 8347 - 8352
反应条件
1: 65 percent / 10percent NaOH / ethanol / 240 h / 0 °C 2: 60 percent / AlCl3, N,N-dimethylaniline / CH2Cl2 / 0.08 h / 5 °C View Scheme
参考文献
Raju, Vegesna S.; Subbaraju, Gottumukkala V.; Manhas, Maghar S.; Kaluza, Zbigniew; Bose, Ajay K.
Tetrahedron, 1992 , vol. 48, # 39 p. 8347 - 8352
反应条件
1: 65 percent / 10percent NaOH / ethanol / 240 h / 0 °C 2: 60 percent / AlCl3, N,N-dimethylaniline / CH2Cl2 / 0.08 h / 5 °C View Scheme
参考文献
Raju, Vegesna S.; Subbaraju, Gottumukkala V.; Manhas, Maghar S.; Kaluza, Zbigniew; Bose, Ajay K.
Tetrahedron, 1992 , vol. 48, # 39 p. 8347 - 8352
反应条件
1: 40 percent / KHCO3 / acetone / Heating 2: 60 percent / triflic acid / 192 h / Ambient temperature 3: 82 percent / K2CO3 / 1,2-dimethoxy-ethane / 12 h / Heating 4: 65 percent / 10percent NaOH / ethanol / 240 h / 0 °C 5: 60 percent / AlCl3, N,N-dimethylaniline / CH2Cl2 / 0.08 h / 5 °C View Scheme
参考文献
Raju, Vegesna S.; Subbaraju, Gottumukkala V.; Manhas, Maghar S.; Kaluza, Zbigniew; Bose, Ajay K.
Tetrahedron, 1992 , vol. 48, # 39 p. 8347 - 8352
