in methanol T=25 - 26°C; 2.1 h; Irradiationexternal 254 nm lamp; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Freeman, Sally; Harger, Martin J. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 571 - 578
Multi-step reaction with 3 steps 1: methanol / 2.1 h / 25 - 26 °C / Irradiation; time dependence of product ratio, intermediate species2: 74 percent / CH2Cl2 / 1 h3: methanol / 27 °C / stability under or without UV-irradiation in DMSO
参考文献
Freeman, Sally; Harger, Martin J. P. Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 571 - 578
