2-氨基-4-氯-7h-吡咯并[2,3-d]嘧啶-5-甲腈合成路线 (共 4 条)
反应条件
triethylamine; trichlorophosphate in acetonitrile T=65 - 95°C;
参考文献
Wilding, Birgit; Winkler, Margit; Petschacher, Barbara; Kratzer, Regina; Glieder, Anton; Klempier, Norbert
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 11-12 p. 2191 - 2198
反应条件
N,N-diethylaniline; trichlorophosphate Heating;
参考文献
Ramasamy; Robins; Revankar
Journal of the Chemical Society - Series Chemical Communications, 1989 , # 9 p. 560 - 562
反应条件
1: 65 percent / triethylamine (TEA) / dimethylformamide 2: 73 percent / NH3 / methanol / 120 °C 3: 40 percent / POCl3, N,N-diethylaniline (DEA) / Heating View Scheme
参考文献
Ramasamy; Robins; Revankar
Journal of the Chemical Society - Series Chemical Communications, 1989 , # 9 p. 560 - 562
反应条件
1: 73 percent / NH3 / methanol / 120 °C 2: 40 percent / POCl3, N,N-diethylaniline (DEA) / Heating View Scheme
参考文献
Ramasamy; Robins; Revankar
Journal of the Chemical Society - Series Chemical Communications, 1989 , # 9 p. 560 - 562