2-[3-(二异丙胺基)-1-苯丙基l]-4-甲基苯酚合成路线 （共 23 条）
反应条件
1: feso chromenyl With titanium (IV) isopropoxide in tetrahydrofuran 1 h; Reflux; 2: diisopropylamine With sodium cyanoborohydride T=70°C;
参考文献
Organic Process Research and Development, , vol. 15, # 5 p. 1010 - 1017
反应条件
1: feso chromenyl With titanium (IV) isopropoxide in tetrahydrofuran 1 h; Reflux; 2: diisopropylamine With sodium tetrahydroborate T=20°C;
参考文献
Organic Process Research and Development, , vol. 15, # 5 p. 1010 - 1017
反应条件
1.1: 1-methyl-piperazine / toluene / Heating 1.2: 5 h / Reflux 2.1: titanium (IV) isopropoxide / tetrahydrofuran / 1 h / Reflux 2.2: 70 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 15, # 5 p. 1010 - 1017
反应条件
1.1: 1-methyl-piperazine / toluene / Heating 1.2: 5 h / Reflux 2.1: titanium (IV) isopropoxide / tetrahydrofuran / 1 h / Reflux 2.2: 70 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 15, # 5 p. 1010 - 1017
反应条件
1: hydrogen; [RhCl(η2:η2-cycloocta-1,5-diene)]2 / toluene / 72 h / 100 °C / 76005.1 Torr 2: 5 palladium on charcoal / toluene / 72 h / 50 °C / |Inert atmosphere; |Molecular sieve 3: platinum(IV) oxide; hydrogen / 24 h / 120 °C / 60804.1 Torr View Scheme
参考文献
Organic Process Research and Development, , vol. 6, # 4 p. 379 - 383
反应条件
1: activated acid alumina S / 1,2-dichloro-benzene / 72 h / |Reflux 2: hydrogen; [RhCl(η2:η2-cycloocta-1,5-diene)]2 / toluene / 72 h / 100 °C / 76005.1 Torr 3: 5 palladium on charcoal / toluene / 72 h / 50 °C / |Inert atmosphere; |Molecular sieve 4: platinum(IV) oxide; hydrogen / 24 h / 120 °C / 60804.1 Torr View Scheme
参考文献
Organic Process Research and Development, , vol. 6, # 4 p. 379 - 383
反应条件
1: activated acid alumina S / 1,2-dichloro-benzene / 72 h / |Reflux 2: hydrogen; [RhCl(η2:η2-cycloocta-1,5-diene)]2 / toluene / 72 h / 100 °C / 76005.1 Torr 3: 5 palladium on charcoal / toluene / 72 h / 50 °C / |Inert atmosphere; |Molecular sieve 4: platinum(IV) oxide; hydrogen / 24 h / 120 °C / 60804.1 Torr View Scheme
参考文献
Organic Process Research and Development, , vol. 6, # 4 p. 379 - 383
反应条件
1.1: 3 h / Reflux 2.1: potassium hydroxide / 1.5 h / 100 - 105 °C 2.2: 4 h / 140 - 145 °C 3.1: AlCl3, aluminium chloride / dichloromethane / 10 - 25 °C View Scheme
参考文献
Synthetic Communications, , vol. 41, # 11 p. 1565 - 1571
反应条件
1.1: triethylamine 2.1: 3 h / Reflux 3.1: potassium hydroxide / 1.5 h / 100 - 105 °C 3.2: 4 h / 140 - 145 °C 4.1: AlCl3, aluminium chloride / dichloromethane / 10 - 25 °C View Scheme
参考文献
Synthetic Communications, , vol. 41, # 11 p. 1565 - 1571
反应条件
1.1: 3 h / Reflux 2.1: potassium hydroxide / 1.5 h / 100 - 105 °C 2.2: 4 h / 140 - 145 °C 3.1: AlCl3, aluminium chloride / dichloromethane / 10 - 25 °C View Scheme
参考文献
Synthetic Communications, , vol. 41, # 11 p. 1565 - 1571
