反应条件
1.1: 94 percent / Zn; NiCl2*6H2O / tetrahydrofuran; H2O / 3 h / 20 °C
2.1: 99 percent / LiAlH4 / diethyl ether / 5 h / 20 °C
3.1: 99 percent / 48 percent aq. HBr; H2SO4 / 5 h / 135 °C
4.1: Li / diethyl ether / 1 h
4.2: 40 percent / diethyl ether / 20 °C
5.1: 46.4 percent / CrO3; AcOH / 3 h
6.1: 28 percent / Zn; HgCl2; aq. HCl / toluene / 30 h / Heating
7.1: aq. NaOH
View Scheme
参考文献
Gu, Chungang; Wysocki, Vicki H.; Harada, Atsuhiro; Takaya, Hiroaki; Kumadaki, Itsumaro
Journal of the American Chemical Society, 1999 , vol. 121, # 45 p. 10554 - 10562
