反应条件
1: 1.) lithium diisopropylamide / 1.) THF, -78 gradC, 30 min. 2.) CH2Cl2, from -78 gradC to 23 gradC, 1.5 h. 2: titanium tetrachloride / CH2Cl2 / 1 h / 0 °C 3: 1.) 6N HCl, HOAc 2.) propylene oxide / 1.) 100 gradC, 3 h. 2.) EtOH View Scheme
参考文献
Walker, Daniel M.; Logusch, Eugene W.
Tetrahedron Letters, 1989 , vol. 30, # 10 p. 1181 - 1184
