NAlpha-芴甲氧羰基-Nγ-羰-L-2,4-氨基丁酸合成路线 （共 4 条）
反应条件
triethylamine in water; dimethyl sulfoxide
参考文献
Sakura, Naoki; Itoh, Tatsuya; Uchida, Yoshiki; Ohki, Kazuhiro; Okimura, Keiko; Chiba, Kenzo; Sato, Yuki; Sawanishi, Hiroyuki
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 10 p. 1915 - 1924
反应条件
1: 88.9 percent / I,I-bis(trifluoroacetoxy)iodobenzene; H2O / dimethylsulfoxide / 20 h 2: 74.2 percent / triethylamine / H2O; dimethylsulfoxide View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 77, # 10 p. 1915 - 1924
反应条件
1: 88 percent / toluene / 0.25 h / microwave irradiation 2: 73 percent / LiOH / tetrahydrofuran / 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 36, # 19 p. 2901 - 2912
反应条件
1: 94 percent / N-methylmorpholine; IBC-Cl; NaN3 / tetrahydrofuran / 0.5 h / -10 °C 2: 88 percent / toluene / 0.25 h / microwave irradiation 3: 73 percent / LiOH / tetrahydrofuran / 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 36, # 19 p. 2901 - 2912
