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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
125251-42-5
合成路线
（共 24 条）
89343-06-6
三异丙基硅基乙炔
→
反应条件
125251-42-5
反应条件
Hexaiodobenzene; triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) chloride T=59.85°C; 12 h;
参考文献
Constable, Edwin C.; Gusmeroli, Deborah; Housecraft, Catherine E.; Neuburger, Markus; Schaffner, Silvia
Acta Crystallographica Section C: Crystal Structure Communications, 2006 , vol. 62, # 8 p. o505-o509
1015423-92-3
+
22779-05-1
→
反应条件
1269800-65-8
+
125251-42-5
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; (dimethyl)(phenyl)phosphine in 1,3-dimethyl-imidazolidin-2-one T=135°C; 6 h; Inert atmosphere;
参考文献
Arisawa, Mieko; Igarashi, Yui; Tagami, Yoko; Yamaguchi, Masahiko; Kabuto, Chizuko
Tetrahedron Letters, 2011 , vol. 52, # 8 p. 920 - 922
821-09-0
4-戊烯-1-醇
→
反应条件
125251-42-5
+
183440-00-8
反应条件
tris-(dibenzylideneacetone)dipalladium(0); bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate in toluene T=65 - 70°C; 4 h; Inert atmosphere;
参考文献
Nicolai, Stefano; Waser, Jerome
Organic Letters, 2011 , vol. 13, # 23 p. 6324 - 6327
696-62-8
4-碘苯甲醚
+
89343-06-6
三异丙基硅基乙炔
→
反应条件
125251-42-5
+
144304-05-2
反应条件
pyrrolidine; [(N-di(2-pyridyl)methyl-N'-cyclohexylurea)PdCl2] in water T=110°C; Sonogashira-Hagihara reaction; 17 h;
参考文献
Najera, Carmen; Gil-Molto, Juan; Karlstroem, Sofia; Falvello, Larry R.
Organic Letters, 2003 , vol. 5, # 9 p. 1451 - 1454
53214-97-4
+
159641-97-1
→
反应条件
125251-42-5
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide in tetrahydrofuran T=25°C; Stille coupling; 12 h; Inert atmosphereDarkness;
参考文献
Decicco, Racquel C.; Black, Allison; Li, Lei; Goroff, Nancy S.
European Journal of Organic Chemistry, 2012 , # 25 p. 4699 - 4704
1015423-92-3
→
反应条件
629-45-8
二丁基二硫
+
125251-42-5
反应条件
tris(4-methoxyphenyl)-phosphine; [Rh(H)(PEt3)3] in acetone 2 h; Heating;
参考文献
Arisawa, Mieko; Tagami, Yoko; Yamaguchi, Masahiko
Tetrahedron Letters, 2008 , vol. 49, # 10 p. 1593 - 1597
→
反应条件
反应条件
copper(l) iodide; N-ethyl-N,N-diisopropylamine in ethyl acetate; acetonitrile T=40°C; Huisgen reaction; 72 h; Inert atmosphere;
参考文献
Christensen, Helena Staunstrup; Sigurskjold, Bent W.; Frihed, Tobias Gylling; Marinescu, Lavinia G.; Pedersen, Christian M.; Bols, Mikael
European Journal of Organic Chemistry, 2011 , # 27 p. 5279 - 5290
821-09-0
4-戊烯-1-醇
→
反应条件
反应条件
tris-(dibenzylideneacetone)dipalladium(0); bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate in tetrahydrofuran T=65 - 70°C; 15 h; Inert atmosphere;
参考文献
Nicolai, Stefano; Waser, Jerome
Organic Letters, 2011 , vol. 13, # 23 p. 6324 - 6327
589-87-7
对溴碘苯
+
89343-06-6
三异丙基硅基乙炔
→
反应条件
125251-42-5
+
271242-20-7
反应条件
piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide T=0 - 20°C; Arylation; 17 h;
参考文献
Godt, Adelheid; Uensal, Oemer; Roos, Mark
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2837 - 2842
627-19-0
1-戊炔
+
89343-06-6
三异丙基硅基乙炔
→
反应条件
1236153-63-1
+
125251-42-5
反应条件
copper(I)-USY zeolite; air in N,N-dimethyl-formamide T=110°C; 15 h;
参考文献
Chassaing, Stefan; Alix, Aurelien; Boningari, Thirupathi; Sido, Karim Sani Souna; Keller, Murielle; Kuhn, Philippe; Louis, Benoit; Sommer, Jean; Pale, Patrick
Synthesis, 2010 , # 9 art. no. Z27909SS, p. 1557 - 1567
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