NiBr2(PPh3)2; triphenylphosphine; zinc in acetonitrile T=60 - 65°C; 0.5 h;
参考文献
Chambers, Mark R. I.; Widdowson, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 1365 - 1366
1: triethylamine / PdCl2(PPh3)2 / dimethylformamide / 3 h / 80 °C
2: H2 / Pd-C / ethanol / 1 h
3: 0.22 g / CrO3; H2SO4 / acetone; H2O / 1.33 h
View Scheme
参考文献
Murphy, Paul V.; Hubbard, Rod E.; Manallack, David T.; Wills, Ruth E.; Montana, John G.; Taylor, Richard J. K.
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 12 p. 2421 - 2439
