4-(吡咯烷-1-基)苯-1-磺酰氯合成路线 (共 2 条)
反应条件
oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane T=20°C; 1 h;
参考文献
MEMORY PHARMACEUTICALS CORPORATION
Patent: US2008/200471 A1, 2008 ;
Location in patent: Page/Page column 54 ;
US 20080200471 A1
反应条件
1: SO3, dioxane / 1,2-dichloro-ethane / 1 h / Heating 2: POCl3, 98 percent PCl5 / CH2Cl2 / 4 h / Ambient temperature View Scheme
参考文献
Jur'ew; Arbatskii
Vestnik Moskovskogo Universiteta, 1951 , vol. 6, # 2 p. 97,101
Chem.Abstr., 1952 , p. 8647