(1S,2R,4R)-2-氟-1-异丙基-4-甲基环己烷合成路线 (共 3 条)
反应条件
p-MeC6H4IF2 in dichloromethane T=0°C;
参考文献
Koen, Mark J.; Guyader, Frederic Le; Motherwell, William B.
Journal of the Chemical Society, Chemical Communications, 1995 , # 12 p. 1241 - 1242
反应条件
1.1: sodium hydride / tetrahydrofuran / 10 h / 20 °C 1.2: 97 percent / tetrahydrofuran / 1 h / 20 °C 2.1: 48 percent / 70 percent HF/pyridine; N-iodosuccinimide / CH2Cl2 / 0.5 h / -78 - 0 °C View Scheme
参考文献
Gruber, Matthias; Schmutzler, Reinhard; Ackermann, Michael; Seega, Juergen; Haegele, Gerhard
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 44, p. 109 - 122
反应条件
phenylphosphorous tetrafluoride 12 h; Ambient temperature;
参考文献
Gruber, Matthias; Schmutzler, Reinhard; Ackermann, Michael; Seega, Juergen; Haegele, Gerhard
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 44, p. 109 - 122