[(2R,3R,4R)-2,3,4,5-四羟基戊基](2R)-2-(1H-吲哚-3-基)丙酸酯合成路线 （共 6 条）
反应条件
acetic acid T=50°C; 19 h;
参考文献
Richter, Jeremy M.; Whitefield, Brandon W.; Maimone, Thomas J.; Lin, David W.; Castroviejo, M. Pilar; Baran, Phil S.
Journal of the American Chemical Society, 2007 , vol. 129, # 42 p. 12857 - 12869
反应条件
1: 17.5 mg / 4-pyrrolidinopyridine, DCC / diethyl ether / 5 h / 20 °C 2: 1.5 mg / 1N HCl / tetrahydrofuran / 18 h / 20 °C View Scheme
参考文献
Yoshida, Noriyuki; Sassa, Takeshi
Agricultural and Biological Chemistry, 1990 , vol. 54, # 10 p. 2681 - 2683
反应条件
1: 17.5 mg / 4-pyrrolidinopyridine, DCC / diethyl ether / 5 h / 20 °C 2: 1.5 mg / 1N HCl / tetrahydrofuran / 18 h / 20 °C View Scheme
参考文献
Yoshida, Noriyuki; Sassa, Takeshi
Agricultural and Biological Chemistry, 1990 , vol. 54, # 10 p. 2681 - 2683
反应条件
1: KIO4 2: 1.0 g / LiBH4 / ethanol / 1.5 h / Ambient temperature 3: 17.5 mg / 4-pyrrolidinopyridine, DCC / diethyl ether / 5 h / 20 °C 4: 1.5 mg / 1N HCl / tetrahydrofuran / 18 h / 20 °C View Scheme
参考文献
Yoshida, Noriyuki; Sassa, Takeshi
Agricultural and Biological Chemistry, 1990 , vol. 54, # 10 p. 2681 - 2683
反应条件
1: 17.5 mg / aq. ethanol / 96 h / 26 °C / Acremonium roseum I 4267 2: 17.5 mg / 4-pyrrolidinopyridine, DCC / diethyl ether / 5 h / 20 °C 3: 1.5 mg / 1N HCl / tetrahydrofuran / 18 h / 20 °C View Scheme
参考文献
Yoshida, Noriyuki; Sassa, Takeshi
Agricultural and Biological Chemistry, 1990 , vol. 54, # 10 p. 2681 - 2683
反应条件
1: 1.0 g / LiBH4 / ethanol / 1.5 h / Ambient temperature 2: 17.5 mg / 4-pyrrolidinopyridine, DCC / diethyl ether / 5 h / 20 °C 3: 1.5 mg / 1N HCl / tetrahydrofuran / 18 h / 20 °C View Scheme
参考文献
Yoshida, Noriyuki; Sassa, Takeshi
Agricultural and Biological Chemistry, 1990 , vol. 54, # 10 p. 2681 - 2683
