in tetrahydrofuran; hexane T=20 - 21°C; 2 h; Irradiation;

in methanol T=15°C; 4 h; Irradiation;

in tetrahydrofuran; hexane T=20 - 21°C; 2 h; Irradiation; Mechanism;

T=-196°C; 10 h; Irradiation; Mechanism;

T=15°C; 4 h; Irradiation; Mechanism;

T=15°C; 4 h; Irradiation; Mechanism;

<b>Multi-step reaction with 3 steps<br /> </b>2: 92 percent / H₂ / 10percent Pd/C / methanol / 1034.3 - 1551.4 Torr<br />3: 1.) 50percent HCl, NaNO₂, 2.) NaN₃ / 1.) H₂O, 10 min, 0-5 deg C, 2.) H₂O, 10-15 min<br /> <br /> &nbsp;