2-[2-(甲氧基甲基)苯基]乙醇合成路线 （共 9 条）
反应条件
toluene-4-sulfonic acid in tetrahydrofuran T=28°C; 0.0833333 h;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2325 - 2332
反应条件
methanol in tetrahydrofuran T=25°C; 1 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2325 - 2332
反应条件
methanol in tetrahydrofuran T=25°C; 1 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2325 - 2332
反应条件
1: DIBAL / toluene / 0.08 h / -90 °C 2: 44 percent / HCl / methanol / 10 h / Heating 3: 1) NaH (60percent in paraffin) / 1) THF, 0 deg C, a) 30 min, b) n-pentane, 30 min, 2) 60 deg C, 20 min 4: TsOH / tetrahydrofuran / 0.08 h / 28 °C View Scheme
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2325 - 2332
反应条件
1: 44 percent / HCl / methanol / 10 h / Heating 2: 1) NaH (60percent in paraffin) / 1) THF, 0 deg C, a) 30 min, b) n-pentane, 30 min, 2) 60 deg C, 20 min 3: TsOH / tetrahydrofuran / 0.08 h / 28 °C View Scheme
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2325 - 2332
反应条件
1: 1) NaH (60percent in paraffin) / 1) THF, 0 deg C, a) 30 min, b) n-pentane, 30 min, 2) 60 deg C, 20 min 2: TsOH / tetrahydrofuran / 0.08 h / 28 °C View Scheme
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2325 - 2332
参考文献
Cremeens, Matthew E.; Hughes, Thomas S.; Carpenter, Barry K.
Journal of the American Chemical Society, 2005 , vol. 127, # 18 p. 6652 - 6661
参考文献
Holliman; Mann
Journal of the Chemical Society, 1947 , p. 1634,1639
反应条件
methanol in tetrahydrofuran T=25°C; 1 h; Irradiationvarious tosylhydrazones, other RONa, also without solvent, other amounts of reagent; Product distributionMechanism;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2325 - 2332
