反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '1869643', constants.ctx, '0')">benzophenone anti-oxime</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1813600', constants.ctx, '0')">trifluoromethylsulfonic anhydride</a>; <a href="#" onclick="return RXDsubstances(event, this, '605283', constants.ctx, '0')">triethylamine</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '635760', constants.ctx, '0')">toluene</a> <br />T=-78°C; 0.0833333 h; Inert atmosphere; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '3574513', constants.ctx, '0')">NaCH(COOEt)2</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '635760', constants.ctx, '0')">toluene</a> <br />T=-78 - 20°C; Inert atmosphere; <br />
参考文献
He, Zhiheng; Li, Huanrong; Li, Zhiping Journal of Organic Chemistry, 2010 , vol. 75, # 13 p. 4636 - 4639