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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
125628-96-8
合成路线
（共 7 条）
134610-29-0
→
反应条件
125628-96-8
反应条件
hydrogen bromide; acetic acid in dichloromethane
参考文献
Hoffmann-La Roche Inc.
Patent: US5236952 A1, 1993 ;
2426-87-1
4-苄氧基-3-甲氧基苯甲醛
→
反应条件
125628-96-8
反应条件
1: diethyl ether; tetrahydrofuran / 1 h / 20 °C 2: NaO-tBu; cyclohexanone / toluene / 0.5 h / Heating 3: ammonium formate / 10percent Pd/C / methanol / 0.5 h / Heating 4: 71 percent / 70percent HNO3; AcOH / 0.5 h / 20 °C 5: AlCl3; pyridine / ethyl acetate / 2 h / Heating View Scheme
参考文献
Learmonth, David A.; Vieira-Coelho, Maria A.; Benes, Jan; Alves, Paula C.; Borges, Nuno; Freitas, Ana P.; Soares-da-Silva, Patricio
Journal of Medicinal Chemistry, 2002 , vol. 45, # 3 p. 685 - 695
121-33-5
香草醛
→
反应条件
125628-96-8
反应条件
1: 93 percent / K2CO3 / acetone / 2 h / Heating 2: diethyl ether; tetrahydrofuran / 1 h / 20 °C 3: NaO-tBu; cyclohexanone / toluene / 0.5 h / Heating 4: ammonium formate / 10percent Pd/C / methanol / 0.5 h / Heating 5: 71 percent / 70percent HNO3; AcOH / 0.5 h / 20 °C 6: AlCl3; pyridine / ethyl acetate / 2 h / Heating View Scheme
参考文献
Learmonth, David A.; Vieira-Coelho, Maria A.; Benes, Jan; Alves, Paula C.; Borges, Nuno; Freitas, Ana P.; Soares-da-Silva, Patricio
Journal of Medicinal Chemistry, 2002 , vol. 45, # 3 p. 685 - 695
96306-54-6
→
反应条件
125628-96-8
反应条件
1: ammonium formate / 10percent Pd/C / methanol / 0.5 h / Heating 2: 71 percent / 70percent HNO3; AcOH / 0.5 h / 20 °C 3: AlCl3; pyridine / ethyl acetate / 2 h / Heating View Scheme
参考文献
Learmonth, David A.; Vieira-Coelho, Maria A.; Benes, Jan; Alves, Paula C.; Borges, Nuno; Freitas, Ana P.; Soares-da-Silva, Patricio
Journal of Medicinal Chemistry, 2002 , vol. 45, # 3 p. 685 - 695
96306-72-8
→
反应条件
125628-96-8
反应条件
1: NaO-tBu; cyclohexanone / toluene / 0.5 h / Heating 2: ammonium formate / 10percent Pd/C / methanol / 0.5 h / Heating 3: 71 percent / 70percent HNO3; AcOH / 0.5 h / 20 °C 4: AlCl3; pyridine / ethyl acetate / 2 h / Heating View Scheme
参考文献
Learmonth, David A.; Vieira-Coelho, Maria A.; Benes, Jan; Alves, Paula C.; Borges, Nuno; Freitas, Ana P.; Soares-da-Silva, Patricio
Journal of Medicinal Chemistry, 2002 , vol. 45, # 3 p. 685 - 695
400870-98-6
→
反应条件
125628-96-8
反应条件
pyridine; aluminium trichloride in ethyl acetate 2 h; Heating;
参考文献
Learmonth, David A.; Vieira-Coelho, Maria A.; Benes, Jan; Alves, Paula C.; Borges, Nuno; Freitas, Ana P.; Soares-da-Silva, Patricio
Journal of Medicinal Chemistry, 2002 , vol. 45, # 3 p. 685 - 695
51439-89-5
→
反应条件
125628-96-8
反应条件
1: 71 percent / 70percent HNO3; AcOH / 0.5 h / 20 °C 2: AlCl3; pyridine / ethyl acetate / 2 h / Heating View Scheme
参考文献
Learmonth, David A.; Vieira-Coelho, Maria A.; Benes, Jan; Alves, Paula C.; Borges, Nuno; Freitas, Ana P.; Soares-da-Silva, Patricio
Journal of Medicinal Chemistry, 2002 , vol. 45, # 3 p. 685 - 695
