2,6-二-叔丁基-4-甲基二氮杂乙酸苯酯合成路线 (共 2 条)
反应条件
potassium hydroxide in acetonitrile 24 h; Ambient temperature; Yield given;
参考文献
Doyle, Michael P.; Bagheri, Vahid; Wandless, Thomas J.; Harn, Nancy K.; Brinker, David A.; Eagle, Cassandra T.; Loh, Kuo-Liang
Journal of the American Chemical Society, 1990 , vol. 112, # 5 p. 1906 - 1912
反应条件
1: 76 percent / triethylamine, methanesulfonyl azide / acetonitrile / 1.) reflux, 2.) RT, 7 h 2: 5percent aq. KOH / acetonitrile / 24 h / Ambient temperature View Scheme
参考文献
Doyle, Michael P.; Bagheri, Vahid; Wandless, Thomas J.; Harn, Nancy K.; Brinker, David A.; Eagle, Cassandra T.; Loh, Kuo-Liang
Journal of the American Chemical Society, 1990 , vol. 112, # 5 p. 1906 - 1912