N-丙酰基-(2R)-樟烷-10,2-磺内酰胺合成路线 （共 5 条）
反应条件
sodium hydride in tetrahydrofuran T=0°C;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 39 p. 6829 - 6840
反应条件
triethylamine; lithium chloride in tetrahydrofuran 4 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 60, # 7 p. 2271 - 2273
反应条件
1: H2O2, LiOH / 1.) THF, H2O, 0 deg C 2: 1.) NaH / 1.) toluene, RT, 2 h, 2.) 2 h View Scheme
参考文献
Journal of the American Chemical Society, , vol. 112, # 7 p. 2767 - 2772
反应条件
1: (1S,2R,4R)-2,10-camphorsultam With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: C8H14O3 in tetrahydrofuran; hexane T=-78 - 0°C; 0.75 h; Further stages.;
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 8 p. 1050 - 1060
反应条件
1.1: Et2BOTf; i-Pr2EtN / CH2Cl2; hexane / 0.5 h / -10 °C 1.2: 84 percent / TiCl4 / CH2Cl2; hexane / 2.17 h / -78 °C 2.1: 91 percent / LiOH; H2O2 / tetrahydrofuran; H2O / 1.5 h / 0 °C View Scheme
参考文献
Oppolzer, Wolfgang; Moretti, Robert; Thomi, Silvia
Tetrahedron Letters, 1989 , vol. 30, # 41 p. 5603 - 5606
