Carboetomidate合成路线 (共 2 条)
反应条件
di-tert-butylazodicarboxylate; triphenylphosphine in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
THE GENERAL HOSPITAL CORPORATION; THE BRIGHAM AND WOMEN'S HOSPITAL, INC.; RAINES, Douglas E.; COTTEN, Joseph, F.; FORMAN, Stuart, A.; MILLER, Keith, W.; HUSAIN, Syed, S.; CUNY, Gregory, D.
Patent: WO2011/5969 A2, 2011 ;
Location in patent: Page/Page column 29-30 ;
WO 2011/005969 A2
反应条件
1: di-tert-butylazodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere 2: ethanol; sodium ethanolate / 20 °C View Scheme
参考文献
Laha, Joydev K.; Cuny, Gregory D.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8477 - 8482