1-二苯甲基-3-碘氮杂丁烷合成路线 (共 3 条)
反应条件
potassium iodide in ethylene glycol dimethyl ether; water T=20°C; Reflux;
参考文献
WO2011/61214 A1, ;
Page/Page column 159-160 ;
WO 2011/061214 A1
反应条件
1,3,5-trishydroxybenzene; sodium iodide; sodium nitrite in water; N,N-dimethyl-formamide T=50°C; 48 h;
参考文献
Journal of Organic Chemistry, , vol. 55, # 9 p. 2920 - 2924
反应条件
1: triethylamine / dichloromethane / 1 h / 20 °C 2: potassium iodide / ethylene glycol dimethyl ether; water / 20 °C / Reflux View Scheme
参考文献
WO2011/61214 A1, ;
WO 2011/061214 A1