2-(2-甲氧基乙氧基)-5-(4,4,5,5-四甲基-1,3,2-二噁硼烷-2-基)吡啶合成路线 (共 2 条)
反应条件
potassium acetate; tetrakis(triphenylphosphine) palladium(0) in dimethyl sulfoxide T=80°C; 48 h; Inert atmosphere;
参考文献
EUROSCREEN S.A.; HOVEYDA, Hamid; DUTHEUIL, Guillaume; EL BOUSMAQUI, Mohamed; BERNARD, Jerome
Patent: WO2011/151434 A1, 2011 ;
Location in patent: Page/Page column 51 ;
WO 2011/151434 A1
反应条件
1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C 2: potassium acetate / tetrakis(triphenylphosphine) palladium(0) / dimethyl sulfoxide / 48 h / 80 °C / Inert atmosphere View Scheme
参考文献
EUROSCREEN S.A.; HOVEYDA, Hamid; DUTHEUIL, Guillaume; EL BOUSMAQUI, Mohamed; BERNARD, Jerome
Patent: WO2011/151434 A1, 2011 ;
WO 2011/151434 A1