反应条件
1.1: pyridine / CH2Cl2 / 20 °C 2.1: LiBr / acetone / Heating 3.1: sodium sulfide nonahydrate / ethanol / Heating 4.1: N-chlorosuccinimide / CCl4 / 3 h / Heating 4.2: 20 percent / m-chloroperbenzoic acid / CH2Cl2 / 18 h / 20 °C 5.1: 66 percent / potassium tert-butoxide / tetrahydrofuran; dimethylsulfoxide / 0.17 h / 20 °C View Scheme
参考文献
MaGee; Beck
Journal of Organic Chemistry, 2000 , vol. 65, # 24 p. 8367 - 8371