间-四苯基卟吩-Μ-氧化铁二聚体合成路线 （共 7 条）
反应条件
((C3H7)4N)ClO4 in dichloromethane Electrolysis; 1.0 V ; using platinumbasket working electrode ; electrocatalytical oxidation ; cleavage of dimer ((TPP)Fe)2O;
参考文献
Nanthakumar, Alaganandan; Goff, Harold M.
Inorganic Chemistry, 1989 , vol. 28, p. 4559 - 4561
反应条件
((C3H7)4N)ClO4 in dichloromethane Electrolysis; 1.0 V ; using platinumbasket working electrode ; electrocatalytical oxidation ; cleavage of dimer ((TPP)Fe)2O;
参考文献
Inorganic Chemistry, , vol. 28, p. 4559 - 4561
反应条件
((C3H7)4N)ClO4 in dichloromethane Electrolysis; 1.0 V ; using platinumbasket working electrode ; electrocatalytical oxidation ; cleavage of dimer ((TPP)Fe)2O;
参考文献
Nanthakumar, Alaganandan; Goff, Harold M.
Inorganic Chemistry, 1989 , vol. 28, p. 4559 - 4561
反应条件
hydrogenchloride in dichloromethane equilibration with aq. HCl in a teflon container;; concn. with addn. of heptane;;
参考文献
Hickman, David L.; Nanthakumar, Alaganandan; Goff, Harold M.
Journal of the American Chemical Society, 1988 , vol. 110, # 19 p. 6384 - 6390
反应条件
hydrogen bromide in benzene complex shaken with aq. HBr (contg. chloride) in C6H6; evapd., solid taken up with Et2O, filtered, washed, dried (vac.) for hours, obtained as mixt.;
参考文献
Doeff, Marca M.; Sweigart, D. A.
Inorganic Chemistry, 1982 , vol. 21, p. 3699 - 3705
反应条件
ethanethiol in benzene
24 h;
参考文献
Berthold, Thomas; Rehorek, Detlef; Hennig, Horst
Zeitschrift fuer Chemie (Stuttgart, Germany), 1986 , vol. 26, p. 183 - 184
反应条件
in benzene
Irradiation (UV/VIS); photoexcitation (single 532 or 355-nm 25-ps FWHM pulse); determination with picosecond absorption spectroscopy, total yield no more than about 1E-4 (80percent of TPPFe(1+) and TPPFe-O(1-));
参考文献
Guest, C. R.; Straub, K. D.; Hutchinson, J. A.; Rentzepis, P. M.
Journal of the American Chemical Society, 1988 , vol. 110, # 16 p. 5276 - 5280
