3,5-二氯-6-甲基-1,4-噁唑-2-酮合成路线 （共 9 条）
反应条件
triethyl amine hydrochloride in chlorobenzene T=90°C; 3 h;
参考文献
Vanlaer, Sofie; De Borggraeve, Wim M.; Voet, Arnout; Gielens, Constant; De Maeyer, Marc; Compernolle, Frans
European Journal of Organic Chemistry, 2008 , # 15 p. 2571 - 2581
反应条件
in toluene 24 h; Heating;
参考文献
Afarinkia, Kamyar; Bahar, Akmal; Neuss, Judi; Ruggiero, Andrea
Tetrahedron Letters, 2004 , vol. 45, # 21 p. 3995 - 3998
反应条件
in 1,2-dichloro-benzene T=190°C; 4 h; Inert atmosphere;
参考文献
Delaney, Patrick M.; Huang, Jianhui; Macdonald, Simon J. F.; Harrity, Joseph P. A.
Organic Letters, 2008 , vol. 10, # 5 p. 781 - 783
反应条件
hydrogenchloride T=20°C; 2 h;
参考文献
Afarinkia, Kamyar; Bahar, Akmal; Bearpark, Michael J.; Garcia-Ramos, Yesica; Ruggiero, Andrea; Neuss, Judi; Vyas, Maushami
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9529 - 9537
反应条件
in toluene T=110°C; Cycloaddition; Hetero Diels-Alder reaction; 5 h;
参考文献
De Borggraeve, Wim; Rombouts, Frederik; Van Der Eycken, Erik; Hoornaert, Georges J.
Synlett, 2000 , # 5 p. 713 - 715
反应条件
aluminium trichloride in dichloromethane 2 h; Ambient temperature;
参考文献
Rogiers, Joeri; Wu, Xiujuan; Toppet, Suzanne; Compernolle, Frans; Hoornaert, Georges J
Tetrahedron, 2001 , vol. 57, # 43 p. 8971 - 8981
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene Substitution; Heating;
参考文献
Wu, Xiujuan; Dubois, Kristof; Rogiers, Joeri; Toppet, Suzanne; Compernolle, Frans; Hoornaert, Georges J.
Tetrahedron, 2000 , vol. 56, # 19 p. 3043 - 3051
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene Stille coupling; 24 h; Heating;
参考文献
Afarinkia, Kamyar; Bahar, Akmal; Neuss, Judi; Ruggiero, Andrea
Tetrahedron Letters, 2004 , vol. 45, # 21 p. 3995 - 3998
Title/Abstract Full Text View citing articles Show Details
Afarinkia, Kamyar; Bahar, Akmal; Bearpark, Michael J.; Garcia-Ramos, Yesica; Ruggiero, Andrea; Neuss, Judi; Vyas, Maushami
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9529 - 9537
反应条件
1: SnCl4 / CH2Cl2 / 12 h
2: 91 percent / CHCl3 / Heating
3: 96 percent / H2; K2CO3 / Pd/C / methanol; tetrahydrofuran / 3 h
View Scheme
参考文献
Van der Eycken, Erik; Jidong, Zhang; Kilonda, Amuri; Compernolle, Frans; Toppet, Suzanne; Hoornaert, Georges; Van der Auweraer, Mark; Jackers, Carine; Verbouwe, Wouter; De Schryver, Frans C.
Journal of the Chemical Society. Perkin Transactions 2, 2002 , # 5 p. 928 - 937
