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乙二醇
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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1259092-05-1
合成路线
(共 8 条)
1259092-05-1
+
10365-98-7
3-甲氧基苯硼酸
→
反应条件
10540-43-9
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Wang, Zhan-Yong; Ma, Qin-Na; Li, Ren-Hao; Shao, Li-Xiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7899 - 7906
1259092-05-1
+
1765-93-1
4-氟苯硼酸
→
反应条件
398-23-2
4,4'-二氟联苯
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 45 p. 7899 - 7906
1259092-05-1
+
98-80-6
苯硼酸
→
反应条件
324-74-3
4-氟联苯
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 45 p. 7899 - 7906
1259092-05-1
→
反应条件
324-74-3
4-氟联苯
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 45 p. 7899 - 7906
1259092-05-1
+
5720-05-8
4-甲基苯硼酸
→
反应条件
72093-43-7
4-氟-4-甲基-1,1-联苯
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Wang, Zhan-Yong; Ma, Qin-Na; Li, Ren-Hao; Shao, Li-Xiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7899 - 7906
1259092-05-1
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
66175-47-1
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Wang, Zhan-Yong; Ma, Qin-Na; Li, Ren-Hao; Shao, Li-Xiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7899 - 7906
110-91-8
吗啉
+
1259092-05-1
→
反应条件
4280-40-4
4-(4-氟-苯基)-吗啉
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [Ni0(1,5-cyclooctadiene)2]; sodium t-butanolate in toluene T=20 - 105°C; Inert atmosphere;
参考文献
Ackermann, Lutz; Sandmann, Rene; Song, Weifeng
Organic Letters, 2011 , vol. 13, # 7 p. 1784 - 1786
1259092-05-1
+
13922-41-3
1-萘硼酸
→
反应条件
572-52-1
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Wang, Zhan-Yong; Ma, Qin-Na; Li, Ren-Hao; Shao, Li-Xiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7899 - 7906