5-溴-2-甲基噻吩-3-羧酸甲酯合成路线 （共 3 条）
反应条件
N-bromosuccinmide; acetic acid in N,N-dimethyl-formamide T=0 - 20°C;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 18 p. 5417 - 5422
反应条件
1: sulfuric acid / Reflux 2: N-bromosuccinmide; acetic acid / N,N-dimethyl-formamide / 0 - 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 18 p. 5417 - 5422
反应条件
1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C 1.2: -78 - 20 °C 2.1: sulfuric acid / Reflux 3.1: N-bromosuccinmide; acetic acid / N,N-dimethyl-formamide / 0 - 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 18 p. 5417 - 5422
