(4R-cis)-6-氰甲基-2,2-二甲基-1,3-二氧六环-4-乙酸叔丁酯合成路线 （共 25 条）
反应条件
Ra-Ni; ammonia; hydrogen in methanol; toluene T=30 - 40°C; P=2625.26 Torr; 2.5 - 6.5 h;
参考文献
Bolton, Gary Louis; Bowles, Daniel Merritt; Boyles, David Christopher; Howard, Walter Allen; Hutchings, Richard H.; Kennedy, Robert Michael; Park, William Keun-Chan; Poel, Toni-Jo; Song, Yuntao
Patent: US2005/239857 A1, 2005 ;
Location in patent: Page/Page column 83 ;
反应条件
1: 95 percent / H2, ammonia / Molybdenum doped Raney nickel / methanol / 2585.7 Torr 2: 75 percent / pivalic acid / toluene; heptane; tetrahydrofuran / Heating 3: aq. HCl / methanol 4: aq. NaOH / methanol View Scheme
参考文献
Tetrahedron Letters, , vol. 33, # 17 p. 2283 - 2284
反应条件
1: 95 percent / H2, ammonia / Molybdenum doped Raney nickel / methanol / 2585.7 Torr 2: 75 percent / pivalic acid / toluene; heptane; tetrahydrofuran / Heating View Scheme
参考文献
Gupta, Lokesh Kumar
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 2012 , vol. 97, p. 495 - 501,7
Title/Abstract Full Text Show Details
Gupta, Lokesh Kumar
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2012 , vol. 97, p. 495 - 501
反应条件
1: 95 percent / H2, ammonia / Molybdenum doped Raney nickel / methanol / 2585.7 Torr 2: 75 percent / pivalic acid / toluene; heptane; tetrahydrofuran / Heating 3: aq. HCl / methanol View Scheme
参考文献
Gupta, Lokesh Kumar
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 2012 , vol. 97, p. 495 - 501,7
Title/Abstract Full Text Show Details
Gupta, Lokesh Kumar
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2012 , vol. 97, p. 495 - 501
反应条件
1: hydrogen; nickel; ammonia / methanol 2: |Acidic conditions 3: hydrogenchloride; methanol 4: sodium hydroxide / water 5: anhydrous calcium acetate / water View Scheme
参考文献
Gupta, Lokesh Kumar
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 2012 , vol. 97, p. 495 - 501,7
Title/Abstract Full Text Show Details
Gupta, Lokesh Kumar
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2012 , vol. 97, p. 495 - 501
