4-(3,5-双三甲基甲硅烷基苯甲酰氨基)-苯甲酸甲酯合成路线 （共 6 条）
反应条件
triethylamine in benzene
参考文献
Journal of Medicinal Chemistry, , vol. 33, # 5 p. 1430 - 1437
反应条件
1: 56 percent / Mg / tetrahydrofuran 2: 77 percent / AlCl3 / CS2 / 1 h / 0 °C 3: 33 percent / Ca(OCl)2, K2CO3, KOH / H2O / 7.5 h / 110 °C 4: SOCl2, CaCO3 / benzene; dimethylformamide / 2 h / Ambient temperature 5: 36 percent / Et3N / benzene View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 33, # 5 p. 1430 - 1437
反应条件
1: 77 percent / AlCl3 / CS2 / 1 h / 0 °C 2: 33 percent / Ca(OCl)2, K2CO3, KOH / H2O / 7.5 h / 110 °C 3: SOCl2, CaCO3 / benzene; dimethylformamide / 2 h / Ambient temperature 4: 36 percent / Et3N / benzene View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 33, # 5 p. 1430 - 1437
反应条件
1: SOCl2, CaCO3 / benzene; dimethylformamide / 2 h / Ambient temperature 2: 36 percent / Et3N / benzene View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 33, # 5 p. 1430 - 1437
反应条件
1: 33 percent / Ca(OCl)2, K2CO3, KOH / H2O / 7.5 h / 110 °C 2: SOCl2, CaCO3 / benzene; dimethylformamide / 2 h / Ambient temperature 3: 36 percent / Et3N / benzene View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 33, # 5 p. 1430 - 1437
反应条件
sodium hydroxide; ethanol
参考文献
Journal of Medicinal Chemistry, , vol. 33, # 5 p. 1430 - 1437
