反应条件
in Petroleum ether
Kinetics; byproducts: C2H6, HCl; (Ar); using Schlenk techniques; addn. of TBP (12 equiv.) to soln. of NdCl3*6H2O (1 equiv.); stirring at 20°C for 10 min, heating at 40°C for 20 min, addn. of soln. of (C2H5)AlCl2 (12 equiv.) in petroleum ether; stirring for 45 s; not isolated, detected with use of luminescence spectroscopy, IR and NMR;
参考文献
Bulgakov, Ramil G.; Kuleshov, Sergei P.; Zuzlov, Aleksei N.; Mullagaleev, Ildar R.; Khalilov, Leonard M.; Dzhemilev, Usein M.
Journal of Organometallic Chemistry, 2001 , vol. 636, # 1-2 p. 56 - 62
