反应条件
byproducts: H2, PH3; dropwise addn. of the phosphate to heated and stirred diborane at 80-105°C over 2 h, heating to 110°C at 1,5 h, all steps under air and moisture exclusion; monitored by NMR;
参考文献
Koester, Roland; Schuessler, Wilhelm; Synoradzki, Ludwik
Chemische Berichte, 1987 , vol. 120, p. 1105 - 1116